In this paper, red mud-based geopolymer microspheres (RM@GMs: 75-150 µm) was prepared by dispersion-suspension-solidification method to remove fluoride ions (F). It was found that RM@GMs still had good mechanical properties and better F removal effect at RM content reached 80 % of the total solid mass. The batch adsorption experiment results showed that the F concentration (< 1.
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