The aim of this study is to prepare hybrid polymer-ceramic dental materials for chairside computer-aided design/computer-aided manufacturing (CAD/CAM) applications. The hybrid polymer-ceramic materials were fabricated via infiltrating polymerizable monomer mixtures into sintered hydroxyapatite/bioactive glass (HA/BAG) ceramic blocks and thermo-curing. The microstructure was observed by scanning electron microscopy and an energy-dispersive spectrometer.
View Article and Find Full Text PDFObjective: To fabricate indirect restorative composites for CAD/CAM applications and evaluate the mechanical properties.
Methods: Polymer-infiltrated-ceramic composites were prepared through infiltrating polymer into partially sintered sodium aluminum silicate ceramic blocks and curing. The corresponding samples were fabricated according to standard ISO-4049 using for mechanical properties measurement.
Objective: The aim of this study was to evaluate the microstructure and mechanical behavior of polymer-infiltrated zirconia ceramics as a function of pre-sintering temperature (1000-1150°C).
Methods: Polymer-infiltrated zirconia ceramics were prepared by combining the porous zirconia networks and polymer through infiltration and polymerization. XRD was employed to determine phase structure.
Objective: To evaluate the microstructure and mechanical behavior of polymer-infiltrated zirconia ceramics as a function of FeO concentration (0-0.3mol%).
Methods: Polymer-infiltrated zirconia ceramics with different concentrations of FeO were prepared by infiltration and polymerization.
Composite ceramics BaTiO₃/3Y-TZP containing 0 mol %, 3 mol %, 5 mol %, 7 mol %, and 10 mol % BaTiO₃ have been prepared by conventional sintering and spark-plasma sintering (SPS), respectively. Analysis of the XRD patterns and Raman spectra reveal that the phase composition of -ZrO₂, -ZrO₂, and BaTiO₃ has been obtained. Our results indicate that SPS can be effective for the decrease in grain size and porosity compared with conventional sintering, which results in a lower concentration of -ZrO₂ and residual stress.
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