Cobalt oxide, nickel oxide and cobalt/nickel binary oxides were synthesised by electrodeposition. To fine tune composition of CoNi alloys, growth parameters including voltage, electrolyte pH/concentration and deposition time were varied. These produced nanomaterials were used as binder free electrodes in supercapacitor cells and tested using three electrode setup in 2 MKOH aqueous electrolyte.
View Article and Find Full Text PDFCobalt nanowires have been synthesized by electrochemical deposition using track-etched anodized aluminum oxide (AAO) templates. Nanowires with varying spacing-to-diameter ratios were prepared, and their magnetic properties were investigated. It is found that the nanowires' easy magnetization direction switches from parallel to perpendicular to the nanowire growth direction when the nanowire's spacing-to-diameter ratio is reduced below 0.
View Article and Find Full Text PDFIn this paper, we report a one-pot chemical synthesis technique for the preparation of iron and iron-carbide nanoparticles. Mössbauer spectroscopy, X-ray diffraction and magnetometry were used as the main tools to identify the different phases of Fe-C present. The influence of experimental parameters on the structural and compositional properties of nanoparticles was investigated in detail.
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