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View Article and Find Full Text PDFComparative investigation of the electrochemical oxygen evolution reaction (OER) activity for clean energy production was performed by fabricating three different electrodes, namely, NiSe, CoSe, and CoNiSe, synthesized by hydrothermal treatment. Cubic, orthorhombic, and hexagonal structures of NiSe, CoSe, and CoNiSe were confirmed by X-ray diffraction (XRD) and also by other characterization studies. Perfect nanospheres, combination of distorted nanospheres and tiny nanoparticles, and sharp-edge nanostructures of NiSe, CoSe, and CoNiSe were explored by surface morphological images.
View Article and Find Full Text PDFInvestigation on the formation mechanism of the β-NiS@Ni(OH) nanocomposite electrode for electrochemical water splitting application was attempted with the use of the hydrothermal processing technique. Formation of single-phase β-NiS, Ni(OH) and composite-phase β-NiS@Ni(OH) has been thoroughly analyzed by X-ray diffractometer (XRD) spectra. Three different kinds of morphologies such as rock-like agglomerated nanoparticles, uniformly stacked nanogills, and uniform nanoplates for β-NiS, Ni(OH), and β-NiS@Ni(OH) materials, respectively, were confirmed by SEM images.
View Article and Find Full Text PDFPolyvinylpyrrolidone (PVP)-assisted nanocatalyst preparation was succeeded by employing a controlled solvothermal route to produce efficient electrodes for electrochemical water-splitting applications. BiWO and FeWO nanocatalysts have been confirmed through the strong signature of (113) and (111) crystal planes, respectively. The binding natures of Bi-W-O and Fe-W-O have been thoroughly discussed by employing X-ray photoelectron spectroscopy which confirmed the formation of BiWO and FeWO.
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