A new, to the best of our knowledge, internal reference method has been developed for the study of the upconversion luminescence of nanoparticle suspensions. This method provides correct analysis and comparison of the luminescent signals obtained under different conditions. To excite the echo signals of samples, it is proposed to use the radiation from an optical parametric oscillator at two wavelengths for the simultaneous excitation of the upconversion luminescence of particles and the Raman scattering signal of the medium in the Stokes region of the spectrum.
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