Nanostructured Fe,Co-Codoped MoO₃ Thin Films.

Molybdenum oxide (MoO₃) and Fe,Co-codoped MoO₃ thin films obtained by spray pyrolysis have been in-depth investigated to understand the effect of Co and Fe codoping on MoO₃ thin films. The effect of Fe and Co on the structural, morphological and optical properties of MoO₃ thin films have been studied using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy-dispersive X-ray analysis (EDAX), optical and photoluminescence (PL) spectroscopy, and electropyroelectric methods. The XRD patterns demonstrated the formation of orthorhombic α-MoO₃ by spray pyrolysis.