The use of the sonoluminescence spectroscopy for the determination of main components in concentrated aqueous solution of alkali metal halides is examined. In concentrated RCl solutions (R = Li, Na, K; = 100-600 g · dm) the sonoluminescence intensity is inversely proportional to ultrasound frequency in the range from 2 Hz up to 5 Hz. In the CsCl case the inverse proportionality is disturbed at ultrasound frequencies higher than 3 MHz.
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