CuBiO synthesized by thermolysis of a new Bi(III)-Cu(II) oxalate coordination compound, namely BiCu(CO)·0.25HO, was tested through its integration within carbon nanofiber paste electrode, namely CuBi/carbon nanofiber (CNF), for the electrochemical detection of amoxicillin (AMX) in the aqueous solution. Thermal analysis and IR spectroscopy were used to characterize a CuBiO precursor to optimize the synthesis conditions.
View Article and Find Full Text PDFThe perovskite-type lanthanum ferrite, LaFeO, has been prepared by thermal decomposition of obtained lanthanum ferrioxalate compound precursor, LaFe(CO)·3HO. The oxalate precursor was synthesized through the redox reaction between 1,2-ethanediol and nitrate ion and characterized by chemical analysis, infrared spectroscopy, and thermal analysis. LaFeO obtained after the calcination of the precursor for at least 550-800 °C/1 h have been investigated by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM).
View Article and Find Full Text PDFNanomaterials (Basel)
November 2019
Single-phase Ce-doped BaTiO powders described by the nominal formula BaCeTiO with = 0.005 and 0.05 were synthesized by the acetate variant of the sol-gel method.
View Article and Find Full Text PDFLuminescent europium-doped hydroxylapatite (EuHAp) nanomaterials were successfully obtained by co-precipitation method at low temperature. The morphological, structural and optical properties were investigated by scanning electron microscopy (SEM), transmission electron microscopy (TEM), -ray diffraction (XRD), Fourier Transform Infrared (FT-IR), UV-Vis and photoluminescence (PL) spectroscopy. The cytotoxicity and biocompatibility of EuHAp were also evaluated using MTT (3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide)) assay, oxidative stress assessment and fluorescent microscopy.
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