Investigation of Hybrid Electrodes of Polyaniline and Reduced Graphene Oxide with Bio-Waste-Derived Activated Carbon for Supercapacitor Applications.

Graphene-based materials have been widely studied in the field of supercapacitors. However, their electrochemical properties and applications are still restricted by the susceptibility of graphene-based materials to curling and agglomeration during production. This study introduces a facile method for synthesizing reduced graphene oxide (rGO) nanosheets and activated carbon based on olive stones (OS) with polyaniline (PAni) surface decoration for the development of supercapacitors.

Optimization Conditions of Malachite Green Adsorption onto Almond Shell Carbon Waste Using Process Design.

Almond shell-based biocarbon is a cheap adsorbent for the removal of malachite green, which has been investigated in this work. FT-IR, DRX, and BET were used to characterize almond shell-based biocarbon. The nitrogen adsorption-desorption isotherms analysis results showed a surface area of 120.

Adsorption of Methylene Blue Dye by Cetyltrimethylammonium Bromide Intercalated Polyaniline-Functionalized Montmorillonite Clay Nanocomposite: Kinetics, Isotherms, and Mechanism Study.

In this study, new adsorbents were prepared by modifying a montmorillonite clay (Mt) with cethyltrimethyl ammonium bromide (CTAB) to form CTAB-Mt, followed by a second modification process with polyaniline (PAni) to form PAni@CTAB-Mt by in situ polymerization of aniline. X-ray diffraction (XRD), X-ray fluorescence spectroscopy (XRF), X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TGA), transmission electron microscopy (TEM), cyclic voltammetry (CV) and the Brunauer-Emmett-Teller (BET) technique were used to characterize the samples. These adsorbents were used in a batch process to remove methylene blue (MB) from aqueous solution.

New Hybrid Adsorbents Based on Polyaniline and Polypyrrole with Silicon Dioxide: Synthesis, Characterization, Kinetics, Equilibrium, and Thermodynamic Studies for the Removal of 2,4-Dichlorophenol.

In the current study, polyaniline and polypyrrole with silicon dioxide (PAni:PPy@SiO) were combined to formulate a new adsorbent, which was examined using XRD, TEM, SEM, FTIR, TGA, and BET, and the adsorption kinetics were investigated by UV-vis spectroscopy. The optical band gap was also evaluated. The electrochemical behavior was investigated using cyclic voltammograms.

Facile Synthesis and Electrochemical Characterization of Polyaniline@TiO-CuO Ternary Composite as Electrodes for Supercapacitor Applications.

This research reports the facile, controlled, low-cost fabrication, and evaluation of properties of polyaniline matrix deposited on titanium dioxide and copper(II) oxide ternary-composite (PANI@TiO-CuO)-based electrode material for supercapacitor application. The process involves the preparation of CuO in the presence of TiO to form TiO-CuO by a facile method, followed by in-situ oxidative polymerization of aniline monomer. The structural and physical properties were evaluated based on the results of FTIR spectroscopy, X-ray diffraction (XRD) analysis, X-ray photoelectron spectroscopy (XPS), transmission electron (TEM) and scanning electron (SEM) microscopy, thermogravimetric analysis (TGA), and BET surface areas analysis.

Development, Investigation, and Comparative Study of the Effects of Various Metal Oxides on Optical Electrochemical Properties Using a Doped PANI Matrix.

A comparative study was performed in order to analyze the effect of metal oxide (MO) on the properties of a polymeric matrix. In this study, polyaniline (PANI)@AlO, PANI@TiC, and PANI@TiO nanocomposites were synthesized using in situ polymerization with ammonium persulfate as an oxidant. The prepared materials were characterized by various analytical methods such as X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), thermogravimetric analysis (TGA), UV/visible (UV/Vis) spectroscopy, Fourier-transform infrared spectroscopy (FTIR), and transmission electron microscopy (TEM).

Reactive Insertion of PEDOT-PSS in SWCNT@Silica Composites and its Electrochemical Performance.

Hybrid silica-modified materials were synthesized on glassy carbon (GC) electrodes by electroassisted deposition of sol-gel precursors. Single-wall carbon nanotubes (SWCNTs) were dispersed in a silica matrix (SWCNT@SiO) to enhance the electrochemical performance of an inorganic matrix. The electrochemical behavior of the composite electrodes was tested against the ferrocene redox probe.