Effect of iron concentration on the growth of carbon nanotubes on clay surface.

The successful growth of carbon nanotubes (CNTs) on montmorillonite (MMT) precursors treated with different concentrations of ferric nitrate at 50 °C (MMT(Fe)-50) and 100 °C (MMT(Fe)-100) was achieved via the in situ chemical vapor deposition (CVD) of acetylene. The as-obtained MMT-CNTs composites were characterized using X-ray diffraction, inductively coupled plasma emission spectrometry, scanning electron microscopy, and transmission electron microscopy. All Fe(3+) ions were intercalated into the MMT interlayers at either 50 or 100 °C in the case of [Fe(3+)]/[clay] = 1.